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Attached is the revised EBL water sampling protocol. | believe it remains consistent with
the intent of DEQ’s draft, while making the instructions a little easier to follow for our
contractors. After some discussion here, we eliminated some of the preliminary steps
either because the information would be collected prior to the water sampling event (e.g.,
year home built) or because elements of the plumbing are just outside the scope of an EBL
investigation. | left some comments in that | hope DEQ can address. In particular, we need
contact information for the lab that the contractors may need to coordinate getting the
sampling kits and delivering the collected samples.
ETC will be in the field on Thursday 11/19. If we cannot finalize this in time for that
investigation, they'll discuss returning to collect the water samples on another day.
Linda D. Dykana, FAD.
Environmental Public Health Director
Division of Environmental Health
Michigan Department of Health & Human Services
517.335 8566
dykemal@ michigan gov
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DRAFT — WORK IN PROGRESS
Protocol for Collecting Residential Drinking Water Samples for Lead Analysis
The following protocol will be used by the Michigan Department of Health and Human Services
(MDHHS) to ensure that residential drinking water samples are collected in a systematic,
consistent manner as part of an elevated blood lead (EBL) investigation. The results will be used
to evaluate human exposure and to identify plumbing components that are contributing lead to
household drinking water.
MDHHS will:
. Collect water samples from the kitchen faucet used for drinking and cooking; a
secondary faucet, most likely a bathroom sink; and any additional faucets based on
frequency of use for consumptive purposes.
. Collect two small volume [125 milliliter (mL)] first-draw samples from each cold
faucet to evaluate exposure to lead in drinking water.
. Collect ten large volume [1 liter (L)] sequential samples from the kitchen cold faucet
to identify plumbing components that are contributing lead to the household water
supply.
. Incorporate the results of water testing into the EBL investigation
Before the EBL Inspection
Obtain information about the age of the house and any building additions. Identify if there are
any records of previous water testing in the past two years.
Instruct residents not use any water in the house for any purpose (including toilet flushing} for
at least 6 hours prior to sample ce }
Step 1 — Prior to Sample Collection
Sampling staff should confirm upon arrival at the home that no water has been used in the
home for at least 6 hours prior to sample collection.
. Identify the primary cold kitchen faucet.
. Identify a secondary cold faucet based on use: most likely a bathroom sink.
. Identify any additional cold faucets that are frequently used.
Document each sampling location with digital photos. Note the presence of any potential brass
components or treatment devices, and whether the faucet has an aerator. Document other
noteworthy items for each location such as leaky faucet, rust stained sink, etc. Document any
exposed plumbing in the basement, if possible.
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If a temporary in-line filter is installed on the faucet, use the by-pass lever to collect unfiltered
water samples. A whole house filter does not preclude sampling, as this is a permanent filter
and representative of actual exposure.
Each water sample must be given a unique identification (ID) code that identifies the location of
the faucet, the sample volume, and the order of sample collection.
Faucet location is indicated as follows:
. KF = kitchen faucet, cold
. BF = bathroom faucet, cold
. OF = other faucet, cold (specify type}
The two 125-mL first draw samples are labeled in order of collection P1 and P2. For example,
the ID codes for the bathroom faucet samples would be BF-P1 and BF-P2.
The 10 large volume 1-L sequential samples collected from the kitchen faucet are labeled A1
through A10. For example, the first sequential sample at the kitchen faucet is labeled KF-A1, the
second is labeled KF-A2 ... through KF-A10.
Step 3 - Collect the Small Volume Samples
Before sample collection:
1. Write the assigned ID code on each sample bottle’s green label using a black Ultra
Fine Point Sharpie permanent marker. To ensure clarity for the DEQ lab, draw a slash
mark through each zero, the number one is a straight vertical line (no hat or foot},
and cross each number seven.
2. Next, remove the cap from each bottle and label using a red Fine Point Sharpie
permanent marker. Write ‘1’ on the white cap of the bottle marked as P1; write ‘2’
on the cap of the bottle marked as P2.
3. Complete the Request for Analysis forms for each sample using a pen, pencil or black
Sharpie. If the Lead and Copper analyses is not already selected, mark as 32CC for
the 125-mL samples.
Collect 125-mL samples from all secondary faucets before collecting any samples from the
primary kitchen faucet. Collect the P1 sample as the very first-draw from each faucet, followed
by the P2 sample.
DO NOT REMOVE THE AERATOR IF THERE IS ONE, but make a notation that there is an aerator
present.
Sample collection:
1. Place the P1 bottle under the faucet, open the faucet to produce a moderate, steady
stream and fill the first bottle to the appropriate level. Immediately fill the P2 bottle
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without a break in the stream (do not turn off the faucet between the first and
second bottle unless necessary and do not allow water to run down the drain in
between the first and second bottle if at all possible).
Turn off faucet. Cap each sample bottle making sure to match the P1 sample to the
‘1’ white cap, and the P2 sample to the ‘2’ white cap.
Secure the appropriate request for water analysis form to each bottle (refer to the
example bottle provided for “instructions”) with a rubber band.
Bundle the P1 and P2 samples collected at each faucet (after the proper paperwork
has been banded to each bottle) and secure them together with a single rubber
band.
Step 4 — Collect the Large Volume Samples
After all 125-mL samples have been collected; collect ten sequential 1-L samples from the
kitchen cold faucet.
Before sample collection:
1.
Write the assigned ID code on each sample bottle’s green label using a black Ultra
Fine Point Sharpie permanent marker. To ensure clarity for the DEQ lab, draw a slash
mark through each zero, the number one is a straight vertical line (no hat or foot),
and cross each number seven.
Next, remove the cap from each bottle and label using a red Fine Point Sharpie
permanent marker. Write 1 through 10 on the white caps of the 1-L bottles for the
A1 through A10 sequential samples.
Complete the Request for Analysis forms for each sample using a pen, pencil or black
Sharpie. If the Lead and Copper analyses is not already selected, mark as 36CC for
the 1-L samples.
Sample collection:
1.
Place the Al bottle under the faucet, open the faucet to produce a moderate, steady
stream and fill the first bottle to the appropriate level. Immediately fill bottles A2 to
A10 consecutively without a break in the stream (do not turn off the faucet between
bottles and do not allow water to run down the drain between the bottles).
After all 1-L samples are collected, turn off faucet. Cap each sample bottle making
sure to match the A1 sample to the ‘1’ white cap, the A2 sample to the ‘2’ white cap
and so forth.
Secure the appropriate request for water analysis form to each bottle (refer to the
example bottle provided for “instructions”) with a rubber band.
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All Method Detection Limits shall be performed according to Title 40 of the Code of Federal
Regulations, Part 136, Guidelines Establishing Testing Procedures for the Analysis of Pollutants,
Appendix B, Definition and Procedure for the Determination of the Method Detection Limit.
Analytical quality control will be in accordance with SOP #800 Revision #4.
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